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ランタン,ユウロピウム,イッテルビウムの空気 : アセチレンフレームによるフレーム分光分析
http://hdl.handle.net/2298/10989
http://hdl.handle.net/2298/10989dd36a807-d239-4705-a41c-f4bcdf5215d0
名前 / ファイル | ライセンス | アクション |
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0525-1931v24_579.pdf (359.9 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2009-02-27 | |||||
タイトル | ||||||
タイトル | ランタン,ユウロピウム,イッテルビウムの空気 : アセチレンフレームによるフレーム分光分析 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
主題 | Europium, Flame photometry, Gel chromatography, Lanthanum, Ytterbium | |||||
資源タイプ | ||||||
資源タイプ | journal article | |||||
著者 |
実政, 勲
× 実政, 勲× 野田, 広× 久永, 明× 出口, 俊雄× 永井, 英夫 |
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別言語の著者 |
實政, 勲
× 實政, 勲× Noda, Hiroshi× Hisanaga, Akira× 出口, 俊雄× Nagai, Hideo× 實政, 勲 |
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内容記述 | ||||||
内容記述 | 希土霜元素の相互分離の簡便な判定法の開発を目的として、ランタン、ユウロピウム、イッテルビウムを選び、それらのフレーム分析法を検討した。比較的低温フレームである空気-アセチレンを用いて、ラソタンの一酸化物バンドスペクトル、ユウロピウム、イッテルビウムの原子線スペクトルより、各々、 0.14、0.04、0.06ppm の感度での定量が可能である。 各種の無機酸、ナトリウムイオン、錯化剤として α-ヒドロキシイソ酪酸 (α-HIEA)、及び他の希土類元素の影響を調べた。 α-HIBA を錆化剤として用いたランタン、ユウロピウム、イッテルビウムのゲルクロマトグラフィーを行い、定量に本法を適用して満足すべき結果を得た。 | |||||
内容記述 | ||||||
内容記述 | The flame spectrophotometric behavior of lanthanum (monoxide band spectrum), europium and ytterbium (atomic line spectra) were studied in commonly utilized air-acetylene flame. A Hitachi Model 508 atomic absorption/flame emission spectrophotometer and premixed slot burner were used. Working curves for lanthanum (0~10), europium (0~3), ytterbium (0~5) ppm were obtained under optimum conditions selected. The effects of inorganic acids {(0.05~4)N} on the emission intensities of the three elements were investigated. Nitric acid does not show serious interference. Perchloric acid gives enhancing effects, while hydrochloric and sulfuric acids give depressing effects in moderately high concentrations. Phosphoric acid shows serious interference owing to its background emission. Ytterbium is liable to be influenced by acids. Interferences of coexisting rare earth elements for ytterbium were found to be large, while those for lanthanum and europium were not serious. This method was applied to the examination of a gel-chromatographic separation of lanthanum, europium and ytterbium using α-hydroxyisobutyric acid as a complexing agent. Percent recovery of the three elements ranged from 93 to 104%. The present method is rapid and simple, and applicable to the preliminary examination of any separation method for the rare earth elements. |
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書誌情報 |
分析化学 巻 24, 号 9, p. 579-584, 発行年 1975-09-10 |
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書誌レコードID | ||||||
収録物識別子 | AN00222633 | |||||
権利 | ||||||
権利情報 | 社団法人日本分析化学会 | |||||
情報源(ISSN) | ||||||
関連名称 | 05251931 | |||||
フォーマット | ||||||
内容記述 | application/pdf | |||||
形態 | ||||||
359916 bytes | ||||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
日本十進分類法 | ||||||
主題 | 433.57 | |||||
その他の言語のタイトル | ||||||
その他のタイトル | Flame emision spectrophotometoric determination of lanthanum, europium and ytterbium in air-acetylene flame | |||||
タイトル(ヨミ) | ||||||
その他のタイトル | ランタン ユウロピウム イッテルビウム ノ クウキ : アセチレン フレーム ニ ヨル フレーム ブンコウ ブンセキ | |||||
出版者 | ||||||
出版者 | 日本分析化学会 | |||||
資源タイプ | ||||||
内容記述 | 論文(Article) | |||||
資源タイプ・ローカル | ||||||
雑誌掲載論文 | ||||||
資源タイプ・NII | ||||||
Journal Article | ||||||
資源タイプ・DCMI | ||||||
text | ||||||
資源タイプ・ローカル表示コード | ||||||
01 | ||||||
URL | ||||||
内容記述 | http://www.jsac.or.jp/bunka/bunsekikagaku.html |