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Dihydropyrene annelated with dihydrothieno[3.4-b]pyrazine: synthesis and photoswitching property
http://hdl.handle.net/2298/16912
http://hdl.handle.net/2298/169120209a276-b62f-46ac-aaef-181bfad3b3dc
名前 / ファイル | ライセンス | アクション |
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TL_51(2010)_4033-4036r.pdf (287.6 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2010-11-18 | |||||
タイトル | ||||||
タイトル | Dihydropyrene annelated with dihydrothieno[3.4-b]pyrazine: synthesis and photoswitching property | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ | journal article | |||||
著者 |
澤田, 剛
× 澤田, 剛× 黒木, 瑞恵× 小川, 智也× 下城, 健太朗× 地福, 寿史× 伊原, 博隆 |
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別言語の著者 |
澤田, 剛
× 澤田, 剛× 黒木, 瑞恵× 小川, 智也× 下城, 健太朗× 地福, 寿史× 伊原, 博隆 |
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内容記述 | ||||||
内容記述 | In this study, 9,10-diacetoxyl-2,7-di-tert-butyl-trans-10b,10c-dimethyl-10b,10c-dihydropyrene annelated with a dihydrothieno[3.4-b]pyrazine unit (1a) was prepared, for the first time, from 5,13-di-tert-butyl-8,16-dimethyl-1,2,9,10- tetrahydroxy[2.2]metacyclophane and 3,4-diaminothiophene in two steps. The photoisomerization property of 1 was investigated by UV and 1H-NMR spectroscopies, and the quantitative isomerization between the more stable dihydropyrene (DHP) form and the less stable metacyclophane-diene (MCPD) form was observed. A thermally induced return reaction from the MCPD to the DHP form was examined at various temperatures, and the reaction rate was 0.0049 min-1 at 45°C, which is slower than that of the parent MCPD. | |||||
書誌情報 |
Tetrahedron Letters 巻 51, 号 31, p. 4033-4036, 発行年 2010-08-04 |
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DOI | ||||||
関連タイプ | isVersionOf | |||||
関連識別子 | 10.1016/j.tetlet.2010.05.092 | |||||
権利 | ||||||
権利情報 | ©2010 Elsevier Ltd. | |||||
情報源(ISSN) | ||||||
関連名称 | 00404039 | |||||
フォーマット | ||||||
内容記述 | application/pdf | |||||
形態 | ||||||
287568 bytes | ||||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
日本十進分類法 | ||||||
主題 | 437 | |||||
出版者 | ||||||
出版者 | Elsevier | |||||
資源タイプ | ||||||
内容記述 | 論文(Article) | |||||
資源タイプ・ローカル | ||||||
雑誌掲載論文 | ||||||
資源タイプ・NII | ||||||
Journal Article | ||||||
資源タイプ・DCMI | ||||||
text | ||||||
資源タイプ・ローカル表示コード | ||||||
01 | ||||||
コメント | ||||||
This is an author version based on a templated by Elsevier. |