{"created":"2023-06-19T09:14:09.950109+00:00","id":26289,"links":{},"metadata":{"_buckets":{"deposit":"ef0e695b-8410-4d33-b284-6fbb1ff951f2"},"_deposit":{"created_by":1,"id":"26289","owners":[1],"pid":{"revision_id":0,"type":"depid","value":"26289"},"status":"published"},"_oai":{"id":"oai:kumadai.repo.nii.ac.jp:00026289","sets":["413:414","585:612:1261"]},"author_link":["157791","157783","157792","157793","157790","157786","157785","157787","157630","157794","157782","157788","157784"],"item_15_alternative_title_22":{"attribute_name":"その他の言語のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"A simple 18F-Acetate Synthesis and Purification and Quality Control for Clinical Use"}]},"item_15_alternative_title_23":{"attribute_name":"タイトル（ヨミ）","attribute_value_mlt":[{"subitem_alternative_title":"18F サクサン ノ ヒョウシキ ゴウセイ ト ブンシュ セイセイ リンショウ オウヨウ エノ キソジッケン"}]},"item_15_biblio_info_6":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2012-03-30","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"76","bibliographicPageStart":"71","bibliographicVolumeNumber":"8","bibliographic_titles":[{"bibliographic_title":"熊本大学医学部保健学科紀要"}]}]},"item_15_creator_3":{"attribute_name":"別言語の著者","attribute_type":"creator","attribute_value_mlt":[{"creatorAffiliations":[{"affiliationNameIdentifiers":[{"affiliationNameIdentifier":"","affiliationNameIdentifierScheme":"ISNI","affiliationNameIdentifierURI":"http://www.isni.org/isni/"}],"affiliationNames":[{"affiliationName":"","affiliationNameLang":"ja"}]}],"creatorNames":[{"creatorName":"宮崎, 吉博","creatorNameLang":"ja"},{"creatorName":"ミヤザキ, ヨシヒロ","creatorNameLang":"ja-Kana"},{"creatorName":"Miyazaki, Yoshihiro","creatorNameLang":"en"}],"familyNames":[{"familyName":"宮崎","familyNameLang":"ja"},{"familyName":"ミヤザキ","familyNameLang":"ja-Kana"},{"familyName":"Miyazaki","familyNameLang":"en"}],"givenNames":[{"givenName":"吉博","givenNameLang":"ja"},{"givenName":"ヨシヒロ","givenNameLang":"ja-Kana"},{"givenName":"Yoshihiro","givenNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"157782","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ninomiya, Kentaro"}],"nameIdentifiers":[{"nameIdentifier":"157790","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Takenaga, Eriko"}],"nameIdentifiers":[{"nameIdentifier":"157791","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Yamano, Masaki"}],"nameIdentifiers":[{"nameIdentifier":"157792","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Morishima, Yoshitaka"}],"nameIdentifiers":[{"nameIdentifier":"157793","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Nomori, Hiroaki"}],"nameIdentifiers":[{"nameIdentifier":"157794","nameIdentifierScheme":"WEKO"}]},{"creatorAffiliations":[{"affiliationNameIdentifiers":[{"affiliationNameIdentifier":"","affiliationNameIdentifierScheme":"ISNI","affiliationNameIdentifierURI":"http://www.isni.org/isni/"}],"affiliationNames":[{"affiliationName":"","affiliationNameLang":"ja"}]}],"creatorNames":[{"creatorName":"冨吉, 勝美","creatorNameLang":"ja"},{"creatorName":"トミヨシ, カツミ","creatorNameLang":"ja-Kana"},{"creatorName":"Tomiyoshi, Katsumi","creatorNameLang":"en"}],"familyNames":[{"familyName":"冨吉","familyNameLang":"ja"},{"familyName":"トミヨシ","familyNameLang":"ja-Kana"},{"familyName":"Tomiyoshi","familyNameLang":"en"}],"givenNames":[{"givenName":"勝美","givenNameLang":"ja"},{"givenName":"カツミ","givenNameLang":"ja-Kana"},{"givenName":"Katsumi","givenNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"157630","nameIdentifierScheme":"WEKO"}]}]},"item_15_description_17":{"attribute_name":"フォーマット","attribute_value_mlt":[{"subitem_description":"application/pdf","subitem_description_type":"Other"}]},"item_15_description_46":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"subitem_description":"論文(Article)","subitem_description_type":"Other"}]},"item_15_description_5":{"attribute_name":"内容記述","attribute_value_mlt":[{"subitem_description":"18F-Acetate (18F-Ace) was synthesized by a simple and quick halogen phase exchange catalysis. solvent extraction method was employed to purify 18F-Ace directly from the reaction vessel. These all simple synthesis and purification method make reactions short and quick so that all synthesis time takes less than 30 minutes. 2- Iodo-acetic ethylester (ICH2COOC2H5) dissolved in anhydrous acetylnirile reacted with 18F-fluorine in Kriptfix-222 and produce 2-18F-acetic ethylester in acetylinitrile. Final product 18F-Ace was obtained by hydrolysis of 2-18F-acetic ethylester in 0.25N NaOH. 18F-Actate radiochemical yield was 48.7% ± 5.2% (n-5). Pyrogen test and sterility check were all negative. With these new simple synthesis and quick purification. 18F-Ace will be more employed to diagnose tumors such as well differentiate one then 18FDG.","subitem_description_type":"Other"}]},"item_15_publisher_36":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"熊本大学"}]},"item_15_source_id_7":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"18807151","subitem_source_identifier_type":"ISSN"}]},"item_15_source_id_9":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AA12010572","subitem_source_identifier_type":"NCID"}]},"item_15_subject_20":{"attribute_name":"日本十進分類法","attribute_value_mlt":[{"subitem_subject":"437.5","subitem_subject_scheme":"NDC"}]},"item_15_text_18":{"attribute_name":"形態","attribute_value_mlt":[{"subitem_text_value":"730396 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